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B. Prestridge, and H. Shapiro, / . Am. Chem. Soc. 83, 2057 (1961). 14. G. N a t t a , R. Ercoli, F . Calderazzo, and A . R a b i z z o n i , / . Am. Chem. Soc. 79, 3611 (1957); R. Ercoli, F. Calderazzo, and G. Bernardi, Gazz. Chim. Ital. 89, 809 (1959). 15. E. O. Fischer, W. Hafner, and K. Ôfele, Ber. 9 2 , 3050 (1959). 16. K. A . K o c h e s k o v , A . N . N e s m e y a n o v , M. M. N a d j , and I. M . Rossinskaya, Compt. Rend. Acad. Sci. URSS 26, 54 (1940). 17. Ε. R. Corey, L. F. D a h l , and W .
Am. Chem. Soc. 89, 5074 (1967); M. R o s e n b l u m and B. N o r t h , ibid. 90, 1060 (1968). 35. R. Bruce, K. Moseley, and P. M . Maitlis, Can. J. Chem. 4 5 , 2011 (1967); R. Bruce and P. M . Maitlis, Can. J. Chem. 4 5 , 2018 (1967). 36. P. M. Maitlis and M. L. G a m e s , J. Am. Chem. Soc. 85, 1887 (1963); Chem. & Ind. (London) p. 1624 (1963); P. M. Maitlis, A . Efraty, a n d M . L. G a m e s , / . Organometal. Chem. (Amsterdam) 2, 284 (1964). 37. E. O. Fischer, K. Ôfele, H . Essler, W. Frohlich, J.
Res. 1, 257 (1968). QUESTIONS 1. T h e neutral nitrosyl ligand ( N O ) behaves as a three-electron donor. O n the basis of electronic configuration and coordination number predict the formulas o f the first-row (3d) transition-metal derivatives containing only carbonyl and nitrosyl groups. QUESTIONS 43 2. Suggest possible m e t h o d s for the preparation of stable arylazo derivatives of transition metals. 3 . Phosphorus trifluoride ( P F ) is a ligand which has "back-bonding" abilities similar t o 3 carbon m o n o x i d e , but which forms stronger chemical bonds to transition metals than carbon m o n o x i d e .