Method performance studies for speciation analysis by Philippe Quevauviller

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By Philippe Quevauviller

Provides an summary of modern experiences played by way of quite a lot of EC laboratories which has ended in the release of collaborative initiatives to enhance the state-of-the-art of speciation research in Europe. Discusses the recommendations used, their functionality as utilized to real-case analyses and attainable resources of mistakes.

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E. bound to the matrix in the same way as the unknown) which is preferably labelled (radioactive labelling would allow verification of the recovery) would be necessary. Such materials not being available, the extraction method used should be validated by other independent methods. Supercritical extractions could be the methods of choice. g. for butyltins [34,35], and seem to offer good possibilities for extracting the species without alteration. These various comments clearly underline that validation of extraction procedures has still not been achieved.

Discussions have also been conducted among experts during scientific workshops which were held in Arcachon (France) in 1990 [27] and Rome in 1994 [28,29]. The following considerations are taken from the summary of the round-tables conducted during these workshops [30] and from the literature [31]. g. g. g. g. g. atomic absorption spectrometry (AAS), mass spectrometry (MS), flame photometric detection (FPD), electron capture detection (ECD), etc. Each of these steps includes specific sources of error which have to be evaluated.

G. AAS). g. by heat-induced decay of the species. Except for cold trapping methods (for water analysis), the separation is performed after extraction and suitable clean-up of the extract. g. anion exchange, ion pairing reversed phase liquid Speciation Analysis of Environmental Samples 15 chromatography (LC) or capillary GC), capillary zone electrophoresis or cold trapping. GC has become a powerful tool in the determination of traces of organic compounds. Unfortunately, such developments are not sufficiently applied in speciation analysis.

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