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By John A. Gladysz, Dennis P. Curran, Istvan T. Horvath
Guide of Fluorous Chemistry; Contents; Preface; individuals; 1 Fluorous Chemistry: Scope and Definition; 2 a private View of the historical past of Fluorous Chemistry; three Fluorous Solvents and comparable Media; four options for the restoration of Fluorous Catalysts and Reagents: layout and evaluate; five Ponytails: Structural and digital concerns; 6 Partition Coefficients related to Fluorous Solvents; 7 Separations with Fluorous Silica Gel and similar fabrics; eight mild Fluorous Chemistry -- A User's consultant
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4 Present Scope of Fluorous Chemistry The definitions associated with fluorous chemistry in the preceding sections are so broad (as they should be) that further introductory classifications would be of little use. Rather, readers are directed to Chapters 3–8 for structured treatments of various aspects and protocols. Although Figure 1-1 is pedagogically appealing as a point of introduction, it now represents just one of countless ways to conduct fluorous reactions, and one of several main strategies for the recovery of fluorous catalysts or reagents.
The field now extends from fluorous nanoparticles on the materials side to fluorous peptides and enzymatic reactions on the biological side. It has evolved so far beyond its original incarnation that a review and reassessment of its working vocabulary is needed, as is provided in the following two sections. 2 The Definition of Fluorous Today As noted above, it was initially envisioned that fluorous would be used analogously to aqueous or aqueous media. However usage dictates definitions, and early researchers soon expanded the term to include fluoroalkyl-labeled species, and this sense dominates in current practice.
1982, 54, 2388, and the references in Table 3-3. ; Arif, A. ; Horva´th, I. ; Gladysz, J. A. Organometallics 1998, 17, 707. Horva´th, I. ; Ra´bai, J. Science 1994, 266, 72. ; Lu P. Angew. , Int. Ed. Engl. 1997, 36, 1454; Angew. Chem. 1997, 109, 1605. (b) Laboratory observations of several coworkers of the authors’ group. Atkins, P. W. In Physical Chemistry, Third Edition; W. H. Freeman and Company: New York, 1986; pp 197–198. Lo Nostro, P. Adv. Colloid Interface Sci. 1995, 56, 245. Juliette, J. J.